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О школе рентгенофизиков г. Ростова-на-Дону Посвящается 130-летию открытия рентгеновского излучения

Sh. I. Duymakaev, A. G. Revenko, A. L. Tsvetyansky, Yu. I. Velichko

Аннотация


Рассмотрен вклад рентгенофизиков г. Ростова-на-Дону (школа профессора М.А. Блохина) в развитие теоретических основ и практических приёмов применения рентгеноспектрального анализа (РСА). В обзоре детально рассмотрены особенности подготовки специалистов по РСА в Ростовcком-на-Дону государственном университете – РГУ (с 2006 г. – Южный федеральный университет – ЮФУ) и организации научно-исследовательской работы в этой области в г. Ростов-на-Дону.  В начальный период (1960-1970 гг.) основное внимание уделялось проверке возможностей и совершенствованию новых для рассматриваемого периода способов анализа. Это способ Битти-Брисси, калибровки, стандарта-фона и добавок. дальнейшем приоритетными стали исследования, основанные на применении теоретических оценок матричных эффектов в рентгенофлуоресцентном анализе (РФА) (оценка вклада избирательного возбуждения в интенсивность аналитических линий, оценка влияния гетерогенности пробы и варианты учёта этого влияния на интенсивность аналитических линий для некоторых практических случаев, применение способа теоретических поправок). Развивались и такие направления, как использование рентгеновских спектров, возбуждаемых протонами и ионами; разработка аппаратуры для вариантов РФА с полным внешним отражением первичного излучения, а также - энергодисперсионных спектрометров со вторичными излучателями и применение этой аппаратуры на практике. Отмечен вклад в разработку и внедрение на предприятиях цветной металлургии автоматизированных систем аналитического контроля (АСАК) сотрудников Базовой научно-исследовательской лаборатории рентгеноспектрального анализа (БНИЛРА) при Ростовском университете. Кратко обсуждён вклад исследовательских групп, работавших под руководством М.А. Блохина, Н.Ф. Лосева и их учеников: В.Ф. Волкова, В.И. Чиркова, Ш.И. Дуймакаева, В.В. Друзя, Ю.И. Величко, В.П. Краснолуцкого, А.Л. Цветянского, М.И. Мазурицкого. Рентгенофизики, выпускники РГУ (и ЮФУ), работали в научных и производственных лабораториях Советского Союза, а в настоящее время продолжают работать – в России и других странах.

Ключевые слова: рентгеноспектральный анализ, история, РФА, ЭДРФА, РФА ПВО, возбуждение протонами и ионами, матричные эффекты, способы анализа,  Ростов-на-Дону

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Литература


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Vershinin A.S., Duimakaev Sh.I., Plyusnina L.N., Berseneva N.P., Kolenko L.I. [X-ray spectral analysis of granites and basalts based on coupling equations]. Apparatus and methods of X-ray analysis, 1977, L.: LNPO “Burevestnik”, Issue 19, pp. 39-44. (in Russian).

Bakhtiarov A.V., Blokhin M.A., Meyer V.A. [Study of the background of a shortwave spectrometer according to Cauchois using a high-resolution PPD]. Apparatus and methods of X-ray analysis, 1977, L.: LNPO “Burevestnik”, Issue 19, pp. 118-134. (in Russian).

Duimakaev Sh.I., Kasinov A.B., Shpolyansky A.Ya. [On the influence of the particle size of a binary sample on the intensity of X-ray fluorescence]. Dep. in VINITI. 1977, № 1929-77, 32 с. (in Russian).

Kasinov A.B., Duimakaev Sh.I., Konoplyannikov S.N., Karmanov V.I. [Intensity of X-ray fluorescence of a multicomponent sample with components of two size classes]. Dep. in VINITI. 1977, № 1930-77, 25 с. (in Russian).

Duimakaev Sh.I., Kasinov A.B., Shpolyansky A.Ya. [X-ray fluorescence intensity of a heterogeneous binary sample consisting of components of different sizes]. Apparatus and methods of X-ray analysis, 1977, L.: LNPO “Burevestnik”, Issue 19, pp. 185-196. (in Russian).

Blokhin M.A. Blokhin S.M. [X-ray spectra excited by high-energy ions (review)]. Zavod. lab. [Industrial Laboratory], 1977, vol. 43, no. 12, pp. 1452-1461. (in Russian).

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Sinitsyn V.N., Losev N.F., Volkov V.F. [An analytical complex for quantitative elemental analysis of a substance using X-ray radiation excited by protons and ions]. Abstr. of the Rep. of the All-Union Sci. Conf. "50 Years of Domestic X-ray Instrumentation" and the 12th All-Union Sci. Conf. on X-ray Spectroscopy. L., 1978, pp. 7-8. (in Russian).

Revenko A.G., Pavlinsky G.V., Losev N.F., Afonin V.P. On the X-ray background in the long-wavelength region of the spectrum. Zavod. lab. [Industrial Laboratory], 1970, vol. 36, no. 2, pp. 166-169. (in Russian).

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Smagunova A.N., Belova R.A., Losev N.F. [X-ray spectral determination of copper in copper concentrate of the Sorsk plant]. Zavod. lab. [Industrial Laboratory], 1970, vol. 36, no. 9, pp. 1055-1058. (in Russian).

Smagunova A.N., Losev N.F., Revenko A.G., Mezhevich A.N. [Generalized scheme for the development of methods for X-ray spectral analysis of industrial products]. Abstr. of the Rep. of the 10th All-Union Conf. on X-ray spectroscopy and X-ray analysis, Alma-Ata, 1973, pp. 60-61. (in Russian).

Gurvich Yu.M., Mezhevich A.N., Plotnikov R.I., Rogachev I.M., Smagunova A.N. [Comparison of methods for accounting for pulp density in X-ray spectral analysis]. Apparatus and methods of X-ray analysis, L.: LNPO “Burevestnik”, 1974, Issue 14, pp. 43-52. (in Russian).

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Rozova O.F., Smagunova A.N., Popova V.I., Pavlinsky G.V., Turapov V.M., Bespalova L.L., Losev N.F. [X-ray spectral determination of elements in products of the Achinsk Alumina Refinery]. Zavod. lab. [Industrial Laboratory], 1975, vol. 41, no. 4, pp. 417-420. (in Russian).

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Kalinin B.D., Myasnikova V.M., Baranov A.A., Mezhevich A.N., Plotnikov R.I., Revenko A.G. [Application of the method of theoretical corrections in X-ray spectral analysis of copper-based alloys]. Zavod. lab. [Industrial Laboratory], 1975, vol. 41, no. 11, pp. 1328-1330. (in Russian).

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Gudzikevich L.I., Mezhevich A.N., Nikolaev V.P., Plotnikov R.I., Raksina P.I., Serbin A.Ya., Losev N.F., Pavlinsky G.V., Revenko A.G., Rylova T.Yu., Savchenko O.M., Smagunova A.N., Shestakov V.A. [Development and implementation of rapid XRF methods for copper-nickel production products]. Abstr. of the 11th All-Union Sci. Conf. on X-ray Spectr., Leningrad: SKBRA, 1975, pp. 83. (in Russian).

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Duimakaev Sh.I., Tsvetyansky A.L., Shmytov A.I. [X-ray spectral determination of high element contents by the standard-background method considering the dependence of the scattering coefficient on the chemical composition of the sample]. Abstr. of the Rep. of the All-Union Sci. Conf. "50 years of domestic X-ray instrument making" and the 12th All-Union Sci. Conf. on X-ray spectra. Leningrad, 1978, pp. 20. (in Russian).

Bakalyar V.N., Gavrilov V.I., Alperovich G.I., Blokhin M.A., Baranov I.Ya., Duimakaev Sh.I. [X-ray radiometric and X-ray spectral analysis of ores and enrichment products considering the mineralogical composition of samples]. Abstr. of the Rep. of the All-Union Sci. Conf. "50 years of domestic X-ray instrument making" and the 12th All-Union Sci. Conf. on X-ray spectra. Leningrad, 1978, pp. 29-30. (in Russian).

Velichko Yu.I., Zabrodin A.N. [Using a set of effective wavelengths to simplify calculations of the intensity of X-ray fluorescence excited by monochromatic radiation]. Abstr. of the 13th All-Union Conf. on Roentgen and Electron Spectroscopy. Lvov, 1981, pp. 24-25. (in Russian).

Kasinov A.B., Zabrodin A.N., Velichko Yu.I., Anapalyan S.A. [Methodological support for automated systems for pulp analysis in a flow]. Abstr. of the 13th All-Union Conf. on Roentgen and Electron Spectroscopy. Lvov, 1981, pp. 26-27. (in Russian).

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Tsvetyansky A.L., Baeva E.P., Duimakaev Sh.I. [Study of the dependence of the ratio of intensities of coherently and incoherently scattered X-ray radiation on the value of the mass scattering coefficient of the sample]. Apparatus and methods of X-ray analysis. L.: Mashinostroenie, 1981, Issue 26, pp. 134-138. (in Russian).

Tsvetyansky A.L., Titarenko A.L., Podshibyakin S.A. [Implementation of the ARF-6 analyzer at the enrichment plant of the Bashkir Copper-Sulfur Plant]. Tsvetnaia metallurgiia [Non-ferrous metallurgy]. 1981, no. 15. pp. 32-33. (in Russian).

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Duimakaev Sh.I., Gavrilov V.I., Anapalyan S.A. [Determination of influence coefficients for binary samples in X-ray spectral analysis using theoretical corrections]. Abstr. of the Rep. of the All-Union Sci. Res. "Development of work on the creation of an automated analytical control system in the Non-Ferrous Metallurgia". Moscow, 1983, pp. 31. (in Russian).

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Blokhina G.E., Velichko Yu.I., Semenova E.V., Sotnikov A.V., Basargin N.N., Rozovsky Yu.G. [X-ray spectral determination of precious metals in ores using concentration]. Abstr. of the Rep. of the 4th zonal seminar "X-ray methods of analysis in scientific research and control of production processes". Krasnoyarsk, 1983, pp. 54-56. (in Russian).

Bakalyar V.N., Druz V.V. [A method for pulp analysis using linearized X-ray fluorescence equations]. Abstr. of the Rep. of the 4th zonal seminar "X-ray methods of analysis in scientific research and control of production processes". Krasnoyarsk, 1983, pp. 69-72. (in Russian).

Druz V.V., Duimakaeva T.G., Bakalyar V.N. [A variant of the analysis method with a comparison element based on simplified linearization of X-ray fluorescence equations]. Abstr. of the Rep. of the 4th zonal seminar "X-ray methods of analysis in scientific research and control of production processes". Krasnoyarsk, 1983, pp. 73-75. (in Russian).

Eritenko A.N., Tsvetyansky A.L. [Approximation of the effective wavelength in X-ray fluorescence analysis of films with arbitrary surface density]. Abstr. of the Rep. of the 14th All-Union Conf. on X-ray and Electron Spectr. Irkutsk, 1984, Pt. 2, pp. 108. (in Russian).

Eritenko A.N., Tsvetyansky A.L., Titarenko A.V. [Tabulation of λeff of primary radiation for films with varying surface density] Abstr. of the Rep. of the 14th All-Union Conf. on X-ray and Electron Spectr. Irkutsk, 1984, Vol. 2, pp. 109. (in Russian).

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Tsvetyansky A.L., Golovko S.A., Eritenko A.N., Titarenko A.V., Duimakaev Sh.I. [Software for automated analytical control systems]. Tsvetnaia metallurgiia [Non-ferrous metallurgy], 1985, no. 2, pp. 99-101. (in Russian).

Eritenko A.N., Tsvetyansky A.L. [Program for selecting the optimal set of regressors in X-ray fluorescence analysis]. Zavod. lab. [Industrial Laboratory],1985, vol. 51, no. 9, pp. 31-33. (in Russian).

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Alperovich G.I., Bakalyar V.N., Maiboroda T.Yu., Nevidimkina S.A. [Application of the automated complex CRAB-ZOOM/ISKRA-1256 for the analysis of ores of the Uchaly Mining and Processing Plant]. Abstr. of the Rep. of the 1st All-Union Conf. on X-ray fluorescence analysis. Orel, 1986, pp. 181. (in Russian).

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Duimakaev Sh.I,, Golovko S.A., Tsvetyansky A.L., Nikolsky A.P. [A variant of the method of theoretical corrections with the determination of the coefficients of interelement influences at the “point” of the analyzed sample]. Methods of X-ray spectral analysis. Novosibirsk: Science, 1986, pp. 62-66. (in Russian).

Eritenko A.N., Tsvetyansky A.L., Titarenko A.V. [A two-parameter representation of the effective wavelength of exciting bremsstrahlung and a version of the method of theoretical corrections for X-ray fluorescence analysis of unsaturated emitters]. Zavod. lab. [Industrial Laboratory], 1986, vol. 52, no. 8, pp. 21-25. (in Russian).

Semenova E.B., Bagdasarov K.N., Blokhina G.E. [Application of polystyrene-azo-thiazane-tilion-2.4 for X-ray fluorescence determination of Au and Ag in ore materials]. Zavod. lab. [Industrial Laboratory], 1988, vol. 54, no. 4, pp. 33-35. (in Russian).

Velichko Yu.I. [A method for X-ray spectral fluorescence analysis using fundamental parameters in case incomplete determination of the composition of a multicomponent sample]. Tomsk, 1988, Deposited at VINITI 22.09.88, № 7469-В88, 8 pp. (in Russian).

Semenova E.B., Blokhina G.E., Velichko Yu.I. [Method of X-ray fluorescence testing of wastewater for mercury content]. Zavod. lab. [Industrial Laboratory], 1989, vol. 55, no. 4, pp. 39-41. (in Russian).

Eritenko A.N., Tsvetyansky A.L., Titarenko A.V. [Use of coupling equations in X-ray spectral analysis of unsaturated emitters]. Abstr. of the Rep. of the 1st All-Union Council on X-ray fluorescence analysis. Orel, 1986, pp. 28. (in Russian).

T svetyansky A.L., Eritenko A.N. [X-ray fluorescence analysis of films]. Abstr. of the Rep. of the 2nd All-Union Conf. on X-ray fluorescence analysis. Irkutsk, 1989. pp. 41. (in Russian).

Mikhnov A.Yu., Tsvetyansky A.L., Pogrebnoy V.P. [X-ray spectral determination of Pt in the processing products of spent alumina-platinum catalysts]. Abstr. of the Rep. of the 2nd All-Union Council on X-ray fluorescence analysis. Irkutsk, 1989, pp. 43. (in Russian).

Titarenko A.V., Tsvetyansky A.L., Eritenko A.N. [Preparation of reference samples for X-ray fluorescence analysis]. Analitika i kontrol’[Analytics and control], 2008, vol. 12, no. 1-2, pp. 42-45. (in Russian).

Tsvetyansky A.L., Eritenko A.N., Antonov A.V., Potashnikov A.Ya. [X-ray spectral determination of the Nb/Sn ratio in alloys of technological coatings]. Zavod. lab. [Industrial Laboratory], 1989, vol. 55, no. 6, pp. 28-31. (in Russian).

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Anapalyan S.A., Golovko S.A., Mikhnov A.Yu., Eritenko A.N., Tsvetyansky A.L. [Software and methodological support for X-ray fluorescence analysis]. Tsvetnaia metallurgiia [Non-ferrous metallurgy], 1989, no. 12, pp. 59-62. (in Russian).

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Duimakaev Sh.I., Tsvetyansky A.L., Golovko S.A. [Method of theoretical corrections with a limited number of spectrometric channels and incomplete information on the composition of the calibration sample]. Dep. to VINITI 5.05.80, no. 3623-80. RSU, Rostov-on-Don, 12 pp. (in Russian).

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Krasnolutsky V.P., Lyubimov D.N., Tsvetyansky A.L. [Influence of concentration gradient on the intensity of X-ray intensity of inhomogeneous layers]. Dep. to VINITI 9.04.82, no. 2089-82. Rostov-on-Don. RSU. 11 pp. (in Russian).

Duimakaev Sh.I., Gavrilov V.I., Shpolyansky A.Ya. [Study of the possibilities of using “homogeneous” influence coefficients on the XRF analysis of heterogeneous samples using the method of theoretical corrections]. Abstr. of the Rep. of the 4th zone. seminar "X-ray methods of analysis in scientific research and control of production processes". Krasnoyarsk, 1983, pp. 52-54. (in Russian).

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Gavrilov V.I., Duimakaev Sh.I. [Application of theoretical influence coefficients in XRF analysis of powder materials]. Abstr. of the Rep. of the 14th All-Union Conf. on X-ray and Electron Spectroscopy. Irkutsk, 1984, vol. 2, pp.141. (in Russian).

Duimakaev Sh.I., Kuznetsov V.Yu., Tarnopolsky M.G., Tsvetyansky A.L. [X-ray fluorescence determination of high concentrations in the presence of interfering elements using scattered radiation]. Abstr. of the Rep. of the 4th zone. seminar "X-ray methods of analysis in scientific research and control of production processes". Krasnoyarsk, 1983, pp. 75-77. (in Russian).

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Golovko S.A., Duimakaev Sh.I., Tsvetyansky A.L., Nikolsky A.P. [On the estimation of interelement influence coefficients in X-ray fluorescence analysis by the method of theoretical corrections]. "Modern metallurgical analysis and studies of the chemical composition of materials, metals, and environmental objects". Abstr. of the Rep. of the Ural Conf., Ustinov. 1985, pp. 120-121. (in Russian).

Golovko S.A., Duimakaev Sh.I., Tsvetyansky A.L. [A simplified expression for calculating the relative contribution of selective excitation in X-ray fluorescence analysis]. "Modern metallurgical analysis and studies of the chemical composition of materials, metals, and environmental objects". Abstr. of the Rep. of the Ural Conf., Ustinov, 1985, pp. 120. (in Russian).

Tsvetyansky A.L., Titarenko A.V., Duimakaev Sh.I., Kurbanov R.M. [Taking into account the magnitude of background intensity in X-ray fluorescence analysis]. "Modern metallurgical analysis and studies of the chemical composition of materials, metals, and environmental objects". Abstr. of the Rep. of the Ural Conf., Ustinov, 1985, pp. 197-198. (in Russian).

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Golovko S.A., Duimakaev Sh.I., Tsvetyansky A.L., Nikolsky A.P. [Application of the method of theoretical corrections in case of incomplete information on the composition of the sample]. Abstr. of the Rep. of the 1st All-Union Conf. on XRF analysis. Orel, 1986, pp. 115. (in Russian).

Golovko S.A., Tsvetyansky A.L., Duimakaev Sh.I. Accounting of the selective excitation in the method of theoretical corrections with the determination of influence coefficients by inverse specific intensities. Abstr. of the Rep. of the 15th All-Union Sci. Conf. on Roentgen and Electron Spectroscopy. L.: LNPO "Burevestnik", 1988, pp. 4. (in Russian).

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Naumtsev F.E., Volkov V.F. [Effect of photoelectron sub excitation in XRF analysis of surface layers of solids]. Abstr. of the Rep. of the 2nd All-Union Conf. on X-ray fluorescence analysis. Irkutsk, 1989, pp. 111 (in Russian).

Labazin A.V., Volkov V.F., Mironenko M.Yu. [Processing of spectra using the Bayesian method in energy-dispersive X-ray spectral analysis]. Abstr. of the Rep. of the 2nd All-Union Conf. on X-ray fluorescence analysis. Irkutsk, 1989, pp. 121 (in Russian).

Naumtsev F.E., Volkov V.F. [The effect of photoelectron sub excitation in X-ray fluorescence analysis of ion-implanted layers]. Zavod. lab. [Industrial Laboratory],1990, vol. 56, no. 9, pp. 41-43. (in Russian)

Naumtsev F.E., Volkov V.F. [The effect of sub excitation by scattered radiation in X-ray fluorescence analysis of ion-implanted layers]. Zavod. lab. [Industrial Laboratory],1991, vol. 57, no. 4, pp. 24-26.

Volkov V.F., Eritenko A.N., Krasnopolskaya N.N. Detection limits of heavy elements obtained with K-series x-rays induced by electron accelerator bremsstrahlung. X-Ray Spectrom., 2000, vol. 29, no. 5. pp. 339-342.

Volkov V.F., Eritenko A.N., Krasnopolskaya N.N. [Estimation of detection limits of heavy elements using K-series X-ray spectra excited by bremsstrahlung from electron accelerators]. Scientific Thought of the Caucasus. Appendix. 2000, no. 1(6), pp. 57-64. (in Russian)

Volkov V.F., Losev V.N., Losev N.F., Sinitsyn V.N. [Evaluation of the possibilities and conditions for determining microquantities of elements by their tertiary X-ray fluorescence spectra]. Izvestiya SKNC VSh., 1980, no. 4, pp. 38-45. (in Russian)

Krasnopolskaya N.N., Volkov V.F. [Accounting for particle size and shape of dispersed monolayer samples collected on membrane filters in XRF with monochromatic excitation]. Abstr. of the Rep. of the 14th All-Union Conf. on X-ray and Electron Spectr., Irkutsk, 1984, Pt. 2, pp. 181. (in Russian)

Volkov V.F., Mironenko M.Yu. [Program for calculating the spectral characteristics of tertiary XRF]. Abstr. of the Rep. of the 1st All-Union Conf. on XRF analysis. Orel, 1986, pp. 162. (in Russian)

Volkov V.F., Gerasimov S.A., Losev V.N., Mironenko M.Yu. [Calculation of radiation distribution over the sample surface in spectrometers with secondary emitters]. Apparatus and methods of X-ray analysis, L.: Mashinostroenie, 1987, Issue 36, pp. 84-89. (in Russian)

Mironenko M.Yu., Volkov V.F. [Program for calculating the spectral characteristics of tertiary XRF]. Dep. to VINITI 20.01.87, No. 399-B87, RSU, Rostov-on-Don, 14 pp. (in Russian)

Volkov V.F., Mironenko M.Yu. [The influence of aperture on the spectral characteristics of tertiary XRF]. Dep. to VINITI 20.01.87, No. 400-B87, RSU, Rostov-on-Don, 12 pp. (in Russian)

Losev N.F., Volkov V.F., Mironenko M.Yu. [Methods for increasing the sensitivity of X-ray spectrometers with a semiconductor detector]. Zavod. lab. [Industrial Laboratory], 1988, vol. 54, no. 2, pp. 28-31. (in Russian)

Naumtsev F.E., Volkov V.F., Losev N.F. [The sub excitation effect in XRF of ion-implanted layers]. Zavod. lab. [Industrial Laboratory],1988, vol. 54, no. 4, pp. 30-33. (in Russian)

Eritenko A.N., Volkov V.F., Losev N.F. [Contribution to the intensity of the analytical line of the scattered bremsstrahlung spectrum of the tube in spectrometers with secondary emitters]. Abstr. of the Rep. of the 15th All-Union Conf. on X-ray and Electron Spectr., L.: LNPO "Burevestnik", 1988. P. 24. (in Russian)

Volkov V.F., Losev N.F., Gerasimov S.A., Semenova E.V. [Accounting the background in energy-dispersive X-ray fluorescence analysis of the composition of matter]. Zavod. lab. [Industrial Laboratory],1989, vol. 55, no. 12, pp. 18-20. (in Russian)

Sinitsyn V.N., Volkov V.F., Losev N.F. [Method for increasing the sensitivity of EDXRF substances]. In: Abstr. of the Rep. of the 2nd All-Union Conf. on X-ray fluorescence analysis. Irkutsk, 1989, pp. 58. (in Russian)

Eritenko A.N., Volkov V.F., Losev N.F. [Contribution of the scattered bremsstrahlung spectrum of a spectrometer tube with secondary emitters to the intensity of the analytical line]. Zavod. lab. [Industrial Laboratory], 1989, vol. 55, no. 12, pp. 20-21. (in Russian)

Volkov V.F., Losev N.F. [The influence of sample particle size on the intensity of proton-excited X-ray radiation]. Zavod. lab. [Industrial Laboratory], 1979, vol. 45, no. 6, pp. 516-519. (in Russian)

Bityutskaya L.V., Volkov V.F., Krasnopolskaya N.N., Losev V.N., Losev N.F., Lisenko P.L., Popov V.S., Sinitsyn V.N. [Analysis of environmental objects by X-ray radiation excited by accelerated protons]. Zavod. lab. [Industrial Laboratory], 1979, vol. 45, no. 9, pp. 811-813. (in Russian)




DOI: https://doi.org/10.15826/analitika.2025.29.4.009

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