An Improved Process for the Preparation of the  p -tert-butylcalix[4]arene: from Laboratory-scale Synthesis to Scale-up Development

A. A. Fat'yanova; A. S. Gusak; O. A. Trofimova; P. E. Prokhorova

doi:10.15826/chimtech.2016.3.2.010

An Improved Process for the Preparation of the p-tert-butylcalix[4]arene: from Laboratory-scale Synthesis to Scale-up Development

A. A. Fat'yanova, A. S. Gusak, O. A. Trofimova, P. E. Prokhorova

Abstract

The article describes the synthesis of p-tert-butylcalix[4]arene with different downloads of the starting compounds. The obtained data revealed the dependence of the yield on solvent, time and download amount. The description of technological process and material flows are given in this article.

Keywords

calix[4]arene; formalin; diphenyl ether; p-tert-butylphenol; condensation; efficiency; scalability; synthesis

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References

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DOI: https://doi.org/10.15826/chimtech.2016.3.2.010

Copyright (c) 2016 A. A. Fatyanova, A. S. Gusak, P. E. Prokhorova, O. A. Trofimova

This work is licensed under a Creative Commons Attribution 4.0 International License.

Chimica Techno Acta, 2014-2024
ISSN 2411-1414 (Online)
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