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An Improved Process for the Preparation of the p-tert-butylcalix[4]arene: from Laboratory-scale Synthesis to Scale-up Development

A. A. Fat'yanova, A. S. Gusak, O. A. Trofimova, P. E. Prokhorova

Abstract


The article describes the synthesis of p-tert-butylcalix[4]arene with different downloads of the starting compounds. The obtained data revealed the dependence of the yield on solvent, time and download amount. The description of technological process and material flows are given in this article.

Keywords


calix[4]arene; formalin; diphenyl ether; p-tert-butylphenol; condensation; efficiency; scalability; synthesis

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References


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DOI: http://dx.doi.org/10.15826/chimtech.2016.3.2.010

Copyright (c) 2016 A. A. Fatyanova, A. S. Gusak, P. E. Prokhorova, O. A. Trofimova

© Chimica Techno Acta, 2014-2019
ISSN 2411-1414 (Online), ISSN 2409-5613 (Print)

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