СМАГУНОВА АНТОНИНА НИКОНОВНА − К 85-ЛЕТИЮ СО ДНЯ РОЖДЕНИЯ

A. G. Revenko, Sh. I. Duymakaev

Аннотация


Рассмотрен творческий путь заслуженного деятеля науки РФ, доктора технических наук, профессора А.Н. Смагуновой (13.08.1934 – 04.03.2018). Основные направления её исследований ‒ разработка методик рентгенофлуоресцентного анализа (РФА) разнообразных материалов, изучение влияния крупности частиц порошковых проб на интенсивность рентгеновской флуоресценции, изучение возможностей и выбор оптимальных условий применения отдельных способов РФА, планирование эксперимента при методических исследованиях аналитической химии, разработка и внедрение методик РФА для производственных лабораторий. Обсуждён её вклад в развитие рентгенофлуоресцентного метода анализа (дана наглядная физическая интерпретация эффекта крупности частиц на результаты РФА, изучены составляющие рентгеновского фона гомогенных и гетерогенных образцов в РФА, теоретически и экспериментально оценены возможности и границы применимости классических способов РФА, разработаны методики анализа биологических, медицинских и экологических материалов). Детальное изучение А.Н. Смагуновой процессов сухого и мокрого измельчения  многокомпонентных материалов в различных механических устройствах привело её к практически важному выводу о том, что более перспективным является мокрое измельчение порошковых проб, исключающее эффект обволакивания. Отмечен её существенный вклад в подготовку и публикацию обзоров как по общему состоянию РФА, так и по конкретным областям его применения. Рассмотрена роль А.Н. Смагуновой в подготовке научных кадров, работа преподавателем Иркутского университета, руководство дипломниками и аспирантами. Отмечен вклад в разработку алгоритмов определения метрологических характеристик методик количественного химического анализа.

Ключевые слова: рентгенофлуоресцентный анализ, влияние крупности частиц, разработка методик РФА, метрологические характеристики


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Литература


REFERENCES

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Losev N.F., Smagunova A.N., Obol’janinova V.G., Pavlinskij G.V. [The choice of optimal conditions in the X-ray spectrometric determination of elements using an internal standard]. Vortrage der Tagung «Die Rontgenspektrometrie und ihre Bedeutung als Analysenmethode». [Reports of the conference «X-ray spectrometry and its importance as an analytical method»]. Berlin, 1972, pp. 166-184 (in German).

Obolyaninova V.G., Smagunova A.N., Pavlinsky G.V., Losev N.F. [Selection of optimal conditions for X-ray determination of tantalum by the method of internal standard]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1974, vol. 29, no. 6, pp. 1160-1164 (in Russian).

Savchenko O.M., Obolyaninova V.G., Smagunova A.N., Losev N.F. [Influence of the spectral composition of the primary radiation on the accuracy of X-ray spectral analysis using the internal standard method]. Zavodskaia laboratoriia. [Industrial laboratory], 1975, vol. 41, no. 4, pp. 412-417 (in Russian).

Obolyaninova V.G., Savchenko O.M., Khrenova G.P., Smagunova A.N., Losev N.F., Lontsikh C.B. [The choice of optimal conditions for X-ray analysis by the method of the internal standard and their use in the attestation of standard samples]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1976, vol. 31, no. 12, pp. 2409-2416 (in Russian).

Karpukova O.M., Smagunova A.N., Obolyaninova V.G., Vavilova O.V. [New version of the internal standard method in X-ray analysis and its use in the standard sample certification]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1979, vol. 34, no. 11, pp. 2085-2089 (in Russian).

Obolyaninova V.G., Smagunova A.N., Zakovyrin O.M., Lontsikh C.B. Development of the X-ray fluorescence determination technique for the tin and its use in standard sample certification]. Apparatura i metody rentgenovskogo analiza [Equipment and methods of X-ray analysis], Leningrad, Mashinostroenie Publ., 1980, no. 23, pp. 47-51 (in Russian).

Karpukova O.M., Smagunova A.N., Matsul V.M., Belomestnova N.V. [X-ray spectral analysis of materials by the method of internal standard using a non-optimal reference element]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1986, vol. 41, no. 4, pp. 606-610 (in Russian).

Karpukova O.M., Smagunova A.N., Skribko N.N., Zhargalsaykhan D. [Development of the X-ray spectral analysis techniques for multicomponent materials by the internal standard method]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1992, vol. 47, no. 4, pp. 678-685 (in Russian).

Pavlinsky G.V., Smagunova A.N., Karpukova O.M., Bolormaa O., Dorzh D. Sources of Error in Total Reflection X-Ray Fluorescence Analysis and Error Correction Using the Internal Standard Method. Journal of Analytical Chemistry, 2002, vol. 57, no. 3, pp. 185-193. https://doi.org/10.1023/A:1014427928483

Ondar U.V., Molchanova E.I., Gomul’skaya G.V., Karpukova O.M, Smagunova A.N., Pavlinskii G.V. Development of a Unified X-ray Fluorescence Procedure for Determining Heavy Metals in Biological Materials. Journal of Analytical Chemistry, 2004, vol. 59, no. 8, pp. 715-721. https://doi.org/10.1023/B:JANC.0000037274.85643.4b

Stepanova T.V., Smagunova A.N., Korzhova E.N. [The choice of analytes’ powder-carrier for the preparing calibration samples when analyzing welding fumes using X-ray fluorescence]. Analitika i kontrol' [Analytics and control], 2015, vol. 19, no. 2, pp. 139-145 (in Russian). DOI: http://dx.doi.org/10.15826/analitika.2015.19.2.011

Pashkova G.V., Smagunova A.N., Finkelstein A.L. [Opportunities of X-ray fluorescence analysis of dairy products using a total reflection X-ray fluorescent spectrometer]. Khimiia v interesakh ustoichivogo razvitiia [Chemistry for Sustainable Development], 2011, vol. 19, no. 3, pp. 327-334 (in Russian).

Smagunova A.N., Shestakov V.A. [X-ray fluorescence methods]. Analiticheskaia khimiia metallov platinovoi gruppy: sbornik obzornykh statei [Analytical chemistry of platinum-group metals: review book]. Moscow, 2003. pp. 441-463 (in Russian).

Smagunova A.N., Molchanova E.I. Rentgenofluorestsentnyi analiz mnogokomponentnykh prob s pomoshch'iu uravnenii sviazi: Metodicheskie ukazaniia. [X-ray fluorescence analysis of multicomponent samples using the constraint equations: Guidelines]. Irkutsk, Irkutsk State University Publ., 2011. 44 p. (in Russian).

Molchanova E.I., Obolianinova V.G., Berkovits L.A., Smagunova A.N. [The use of standard samples for calibration in the X-ray fluorescence analysis of sediment]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1995, vol. 50, no. 3, p. 253-257 (in Russian).

Losev N.F., Revenko A.G., Suchorukov B.L, Smagunova A.N., Pavlinskij G.V. [Investigation of the dependence of the background intensity on the excitation conditions and the chemical composition of the samples]. Vortrage der Tagung «Die Rontgenspektrometrie und ihre Bedeutung als Analysenmethode». [Reports of the conference «X-ray spectrometry and its importance as an analytical method»]. Berlin, 1972, pp. 192-215 (in German).

Sukhorukov B., Smagunova A., Pavlinsky G., Losev N. [Investigation of the background composition in the short-wavelength region of the x-ray fluorescence spectrum]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1975, vol. 30, no. 2, p. 372-375 (in Russian).

Smagunova A.N., Molchanova E.I., Usova E.F. [Accounting for the background in the X-ray fluorescence determination of low contents of elements in steels]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1987, vol. 42, no. 10, p. 1797-1807 (in Russian).

Belykh V.V., Smagunova A.N., Kozlov V.A. [Multiple scattered radiation in X-ray radiometric analysis]. Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1994, vol. 49, no. 10, p. 1092-1096 (in Russian).

Smagunova A.N., Ondar U.V., Nikitina V.G., Kozlov V.A. Background Intensity as a Function of the Particle Size of a Radiating Sample in X-ray Fluorescence Spectroscopy. Journal of Analytical Chemistry, 2001, vol. 56, no. 9, p. 833-836. https://doi.org/10.1023/A:1016760413125

Chuparina E.V., Smagunova A.N., Eliseeva L.A. Study of the Processes of Background Formation in the Long-Wavelength Region of X-Ray Spectrum. Journal of Analytical Chemistry, 2015, vol. 70, no. 8, p. 949–955. https://doi.org/10.1134/S1061934815080055

Smagunova A.N., Gunicheva T.N., Karpukova O.M., Kozlov V.A. [X-ray analysis of atmospheric aerosols]. Zavodskaia laboratoriia [Industrial laboratory], 1993. vol. 59, no. 4, pp. 20-27 (in Russian).

Karpukova O.M., Smagunova A.N., Kozlov V.A. Estimation error of sampling atmospheric aerosols. Zavodskaia laboratoriia [Industrial laboratory], 1995. vol. 61, no. 12. pp. 18-20 (in Russian).

Bolormaa O., Karpukova O.M., Rozova O.F., Polonnikova V.V., Reshetnik L.А., Smagunova A.N. [Determination of Zinc in Hair by X-Ray Spectrometry] Zhurnal analiticheskoi khimii [Journal of Analytical Chemistry], 1998. vol. 53. no. 7. pp. 772-775 (in Russian).

Bolormaa O., Karpukova O.M., Gerbish Sh., Dorj D., Smagunova A.N. [Development of procedure of X-ray fluorescence analysis of hair using a spectrometer with full external reflection of the primary radiation]. Analitika i kontrol' [Analytics and control], 1999. vol. 3, no. 3. pp. 27-31 (in Russian).

Smagunova A.N., Rozova O.F., Aprelkova N.F., Belykh L.I., Kireeva A.N., Martynova N.A., Karpukova O.M., Ivanova E.I., Myl’nikova L.I., Ondar U.V., Bazina I.G., Biryukova E.V. [Impact of aluminum plant emissions on soils and plants in the nearby area]. Ecological chemistry. 1999. Issue 8, no. 4. pp. 253-261 (in Russian).

Ondar U.V., Karpukova O.M., Бутаков Э.М., Шитенкова Е.А., Smagunova A.N. [Development of procedures for X-ray fluorescent determination of As in soils and solid waste from the processing of cobalt ore]. Analitika i kontrol' [Analytics and control], 2000. vol. 4, no. 1. pp. 66-71 (in Russian).

Smagunova A.N., Karpukova O.M., Korzhova E.N., Kozlov V.A., Kuznetsova O.V. [Using the X-ray method for the analysis of atmospheric aerosols]. [Optics of the atmosphere and the ocean]. 2002. vol. 15, pp. 641-644 (in Russian).

Kuznetsova O.V., Korzhova E.N., Smagunova A.N., Mukhetdinova A.V., Tomilova O.A., Sizykh Yu.I. Comparison of the Results of Atomic Absorption and X-ray Fluorescence Analysis of Metals in Atmospheric Aerosols. Journal of Analytical Chemistry, 2004. vol. 59, no. 1, pp. 39-44. https://doi.org/10.1023/B:JANC.0000011666.96528.bd

Stavitskaya M.V., Korzhova E.N., Smagunova A.N. Development of a Procedure for the Determination of X-Ray Fluorescence of Metals in Aerosols. Journal of Analytical Chemistry. 2010. vol. 65, no. 12, pp. 1245-1253. https://doi.org/10.1134/S1061934810120087

Pashkova G.V., Smagunova A.N. [Study of sources of errors in the preparation of milk products for non-destructive x-ray fluorescence analysis] Analitika i kontrol’. [Analytics and control], 2011, vol. 15. no. 1, pp. 47-55 (in Russian).

Smagunova A.N., Pashkova G.V. Choice of optimal conditions for X-ray fluorescence analysis of milk products with varying fat content // X-Ray Spectrom. 2013. V. 42, no. 6, pp. 546-551. DOI 10.1002/xrs.2519

Stepanova T.V., Ondar U.V., Korzhova E.N., Tolmacheva V.S., Smagunova A.N. Choice of Optimum Conditions of Emitter Preparation for X-Ray Fluorescence Analysis of Aerosols. Journal of Analytical Chemistry], 2017. vol. 72, no. 2, pp. 163-170. https://doi.org/10.1134/S1061934817020125

Belykh L.I., Malykh Yu.M., Smagunova A.N., Penzina E.E., Kozlov V.A. Estimation of the Sampling Error in the Determination of Benzo[a]pyrene in Organized Gas–Dust Air Emissions. Journal of Analytical Chemistry. 2003. vol. 58, no. 7, pp. 665-672. https://doi.org/10.1023/A:1024760104373

Smagunova A.N., Ondar U.V., Molchanova E.I., Vashukevich H.V., Kozlov V.A., Aprelkova N.G., Boshchenko N.V. X-ray Fluorescence Determination of Heavy Metals in Humic Acids. Journal of Analytical Chemistry. 2004. vol. 59, no. 11, pp. 1066-1072. https://doi.org/10.1023/B:JANC.0000047009.01907.14

Malykh Yu.M., Belykh L.I., Smagunova A.N., Korzhova E.N., Penzina E.E., Kozlov V.A. [Metrological investigations of Benzo[a]pyrene Determination Methods in industrial Emissions from fixed Sources by low-temperature luminescence]. Analitika i kontrol' [Analytics and control], 2002, vol. 6, no. 1, pp. 61-70 (in Russian).


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